Unexpected Result During Fire Resistance Test (final Test)
by DuralM in Workshop > Molds & Casting
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Unexpected Result During Fire Resistance Test (final Test)
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That’s the second part of refractories test. After that test I will choose the best material for my new metal melting furnace project. This particular experiment consists of 2 smaller tests
Proportions for the First Test
![Unexpected results during fire resistance test.avi_snapshot_00.05_[2016.11.15_19.59.12].jpg](/proxy/?url=https://content.instructables.com/FB8/MBVF/IVHQM1ZV/FB8MBVFIVHQM1ZV.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_00.05_[2016.11.15_19.59.12].jpg)
![Unexpected results during fire resistance test.avi_snapshot_00.28_[2016.11.15_19.59.57].jpg](/proxy/?url=https://content.instructables.com/FE3/X0JZ/IVHQM1ZW/FE3X0JZIVHQM1ZW.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_00.28_[2016.11.15_19.59.57].jpg)
During the first test, I made such mixtures:
1. Fire clay – 100%;
2. Fire clay – 40%; Grog – 40%; Graphite dust – 20%
3. Fire clay – 40%; Grog – 50%; Graphite dust – 10%
4. Fire clay 40%; Grog – 50%; Graphite dust – 5%; Mineral wool – 5%
5. Fire clay – 40% Grog – 40%; Graphite dust – 10%; Alabaster – 10%
6. Alabaster – 50%; Sand – 50%;
7. Cement – 50%; Sand – 50%
Drying Into the Oven
![Unexpected results during fire resistance test.avi_snapshot_00.33_[2016.11.15_20.00.10].jpg](/proxy/?url=https://content.instructables.com/FYU/QJ6D/IVHQM202/FYUQJ6DIVHQM202.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_00.33_[2016.11.15_20.00.10].jpg)
I put samples into the oven to dry them:
- 5 hours +50 C° (122F°);
- 2 hours +100+180 C° (212-356 F°);
- 2 hours +250 C° (482 F°).
After the Oven Drying
![Unexpected results during fire resistance test.avi_snapshot_00.43_[2016.11.15_20.00.29].jpg](/proxy/?url=https://content.instructables.com/F15/DECY/IVHQM205/F15DECYIVHQM205.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_00.43_[2016.11.15_20.00.29].jpg)
All samples survived except one. Sample #6 (Alabaster/Sand – 50/50%) was damaged during the air drying.
Testing With a Torch
![Unexpected results during fire resistance test.avi_snapshot_01.09_[2016.11.15_20.01.43].jpg](/proxy/?url=https://content.instructables.com/F20/15CV/IVHQM20B/F2015CVIVHQM20B.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.09_[2016.11.15_20.01.43].jpg)
![Unexpected results during fire resistance test.avi_snapshot_01.15_[2016.11.15_20.01.58].jpg](/proxy/?url=https://content.instructables.com/F2Z/DNWP/IVHQM20K/F2ZDNWPIVHQM20K.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.15_[2016.11.15_20.01.58].jpg)
First part of the test was with gasoline torch. During it samples didn’t get any damages.
Testing in the Melting Furnace
![Unexpected results during fire resistance test.avi_snapshot_01.38_[2016.11.15_20.02.28].jpg](/proxy/?url=https://content.instructables.com/FYV/IXES/IVHQM22T/FYVIXESIVHQM22T.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.38_[2016.11.15_20.02.28].jpg)
![Unexpected results during fire resistance test.avi_snapshot_01.46_[2016.11.15_20.02.46].jpg](/proxy/?url=https://content.instructables.com/FIR/7LK2/IVHQM230/FIR7LK2IVHQM230.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.46_[2016.11.15_20.02.46].jpg)
![Unexpected results during fire resistance test.avi_snapshot_01.54_[2016.11.15_20.02.59].jpg](/proxy/?url=https://content.instructables.com/FMW/Y4TN/IVHQM239/FMWY4TNIVHQM239.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.54_[2016.11.15_20.02.59].jpg)
![Unexpected results during fire resistance test.avi_snapshot_01.59_[2016.11.15_20.03.09].jpg](/proxy/?url=https://content.instructables.com/FDD/E9J6/IVHQM23F/FDDE9J6IVHQM23F.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_01.59_[2016.11.15_20.03.09].jpg)
![Unexpected results during fire resistance test.avi_snapshot_02.57_[2016.11.15_20.04.13].jpg](/proxy/?url=https://content.instructables.com/FPI/5AYM/IVHQM1VN/FPI5AYMIVHQM1VN.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_02.57_[2016.11.15_20.04.13].jpg)
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![Unexpected results during fire resistance test.avi_snapshot_03.16_[2016.11.15_20.04.44].jpg](/proxy/?url=https://content.instructables.com/FGE/4MOW/IVHQM1W0/FGE4MOWIVHQM1W0.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_03.16_[2016.11.15_20.04.44].jpg)
Second part of the test in the smelting furnace was much more destructive. The process took about an hour. In my opinion, the temperature was more than 1200 C° (2192 F°). All samples were damaged. Only the sample #3 got minor damages. Therefore, in this test it’s the best result.
Nevertheless, the sample #7 (cement/sand – 50/50%) was damaged but held the shape. Therefore, I wanted to make one more test where cement could be one of the main ingredients.
Second Test Samples
![Unexpected results during fire resistance test.avi_snapshot_03.29_[2016.11.15_20.05.14].jpg](/proxy/?url=https://content.instructables.com/FK3/IO0W/IVHQM1WH/FK3IO0WIVHQM1WH.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_03.29_[2016.11.15_20.05.14].jpg)
![Unexpected results during fire resistance test.avi_snapshot_03.45_[2016.11.15_20.05.34].jpg](/proxy/?url=https://content.instructables.com/FB1/8COU/IVHQM1WM/FB18COUIVHQM1WM.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_03.45_[2016.11.15_20.05.34].jpg)
During the second test, I made samples:
1. Cement – 50%; Sand – 25%; Grog – 25%;
2. Cement – 50%; Fire clay – 25%; Grog – 25%;
3. Cement – 40%; Sand – 17.5%; Grog – 15; Fire clay – 27.5%;
4. Cement – 22.5%; Sand – 27.5%; Grog – 22.5%; Fire clay – 27.5%;
5. Cement – 22.5%; Sand – 22.5%; Grog – 22.5%; Fire clay – 27.5%; Graphite dust -5%
All steps of the process were the same as in the first experiment.
Melting
![Unexpected results during fire resistance test.avi_snapshot_04.17_[2016.11.15_20.06.36].jpg](/proxy/?url=https://content.instructables.com/F3K/76AI/IVHQM1WU/F3K76AIIVHQM1WU.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_04.17_[2016.11.15_20.06.36].jpg)
![Unexpected results during fire resistance test.avi_snapshot_04.29_[2016.11.15_20.06.52].jpg](/proxy/?url=https://content.instructables.com/FR4/PDC0/IVHQM1XE/FR4PDC0IVHQM1XE.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_04.29_[2016.11.15_20.06.52].jpg)
![Unexpected results during fire resistance test.avi_snapshot_04.38_[2016.11.15_20.07.08].jpg](/proxy/?url=https://content.instructables.com/F4Q/8JTZ/IVHQM1XL/F4Q8JTZIVHQM1XL.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_04.38_[2016.11.15_20.07.08].jpg)
Finally, in the smelting furnace samples started melting. I think that the problem is the sand and the cement.
Final Results
![Unexpected results during fire resistance test.avi_snapshot_04.42_[2016.11.15_20.07.15].jpg](/proxy/?url=https://content.instructables.com/FT5/WKJC/IVHQMAVC/FT5WKJCIVHQMAVC.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_04.42_[2016.11.15_20.07.15].jpg)
![Unexpected results during fire resistance test.avi_snapshot_04.59_[2016.11.15_20.07.38].jpg](/proxy/?url=https://content.instructables.com/FFA/G4DR/IVHQM1YW/FFAG4DRIVHQM1YW.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_04.59_[2016.11.15_20.07.38].jpg)
![Unexpected results during fire resistance test.avi_snapshot_05.07_[2016.11.15_20.07.50].jpg](/proxy/?url=https://content.instructables.com/FCL/K6TI/IVHQM1Z6/FCLK6TIIVHQM1Z6.jpg&filename=Unexpected results during fire resistance test.avi_snapshot_05.07_[2016.11.15_20.07.50].jpg)
I used the river sand and not the silica sand. Silica sand as I now sustain much higher temperatures than river sand.
I’ve made a decision to use fire clay/grog/graphite dust (40/50/10%) in my new furnace.